Efficient Flow Electrochemical Alkoxylation of Pyrrolidine-1-carbaldehyde
نویسندگان
چکیده
منابع مشابه
2-Methoxynaphthalene-1-carbaldehyde
In the title compound, C(12)H(10)O(2), the aldehyde and meth-oxy groups are slightly twisted around the single bonds that join them to the naphthalene ring system. In the crystal structure, mol-ecules are linked through inter-molecular C-H⋯O hydrogen bonds, forming chains running along the c axis.
متن کاملFerrocene-1-carbaldehyde thiosemicarbazone
The asymmetric unit of the title compound, [Fe(C(5)H(5))(C(7)H(8)N(3)S)], consists of two crystallographically independent mol-ecules, A and B. The cyclo-penta-dienyl (Cp) rings in both mol-ecules adopt an eclipsed conformation and are parallel to each other, forming dihedral angles of 2.5 (3) and 1.1 (3)°, respectively. The mean plane of the semicarbazone group is coplanar with the attached Cp...
متن کامل2,6,6-Trimethylcyclohexene-1-carbaldehyde oxime
In the crystal of the title compound C(10)H(17)NO, synthesized by the reaction of β-cyclo-citral with hydroxyl-amine hydro-chloride, inversion-related mol-ecules are linked by a pair of O-H⋯N hydrogen-bonding inter-actions between the oxime functionalities, forming R(2) (2)(6) loops. The molecular conformation is stabilized by intra-molecular methyl C-H⋯N inter-actions. The cyclohexene ring has...
متن کاملFerrocene-1-carbaldehyde 4-ethylthiosemicarbazone
The asymmetric unit of title compound, [Fe(C(5)H(5))(C(9)H(12)N(3)S)], contains two crystallographically independent mol-ecules, A and B. The two cyclo-penta-dienyl (Cp) rings are parallel to each other in both mol-ecules, forming dihedral angles of 2.3 (3) and 1.0 (3)°, respectively, and adopt an eclipsed conformation. The mean plane of the semicarbazone group is twisted slightly away from the...
متن کاملAn Easy‐to‐Machine Electrochemical Flow Microreactor: Efficient Synthesis of Isoindolinone and Flow Functionalization
Flow electrochemistry is an efficient methodology to generate radical intermediates. An electrochemical flow microreactor has been designed and manufactured to improve the efficiency of electrochemical flow reactions. With this device only little or no supporting electrolytes are needed, making processes less costly and enabling easier purification. This is demonstrated by the facile synthesis ...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: Synlett
سال: 2019
ISSN: 0936-5214,1437-2096
DOI: 10.1055/s-0037-1611774